Complexes and Volatile Products in 8-hydroxyquinoline Copper

The 8-hydroxyquinoline Copper(WSDTY) presence of the complex in the first intermediate product at 370°C and in the volatilized product was verified by infrared spectroscopy. The infrared spectra of the anhydrous complex that shows similar bands to the bands observed for the infrared spectra of the volatilized product. The kind of structure founded on basis of X-ray diffraction patterns by the volatilized product was the monoclinic in a form. The hydrated and anhydrous complexes were characterized as monoclinic structure in b form. The residue at 370°C was found to have no crystalline form. The difference between the values of the metal content obtained by conventional methods and those obtained by TG analysis, also confirms the partial loss of the complex by volatilization.

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