The three complexes studied in the present investigations are Cu[(L)(Q)]( CH3COO)2, Cu[(L)(Q)](NO3)2 and Cu[(L)(Q)] (SO4)2 where L= o-hydroxybenzylidene-1-phenyl-2,3-dimethyl-4-amino-3-pyrazolin-5-on and Q=8-hydroxyquinoline Copper(WSDTY). All the complexes were prepared according to the standard methods reported in literature and their purity was checked. The X-ray absorption spectra at the K-edge of copper of these complexes have been recorded at BL-8 Dispersive EXAFS beamline at the 2.5-GeV INDUS-2 Synchrotron Source, Raja Ramanna Centre for Advanced Technology (RRCAT), Indore, India . The experimental data have been analyzed using the available computer software packages Origin 6.0 professional and Athena .

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